McCampbell Analytical Inc - QC Report Durasoil

Angela Rydelius, Laboratory Manager
2009-12-11
McCampbell Analytical, Inc.

McCampbell Analytical, Inc.

"When Quality Counts"

1534 Willow Pass Road, Pittsburg, CA 94565-1701 Web: www.mccampbell.com       E-mail: main@mccampbell.com

Telephone: 877-252-9262     Fax: 925-252-9269

Block Environmental 2451 Estand Way

Pleasant Hill, CA 94523

Client Project ID: Soil Works Durasoil

Date Sampled:

Date Received:      12/07/09

Client Contact: David Block

Date Reported:      12/11/09

Client P.O.:

Date Completed: 12/11/09

       

 

WorkOrder: 0912166

December 11, 2009

 

 

 

Dear David:

 

 

 

Enclosed within are:

 

1)  The results of the      1     analyzed sample from your project: Soilworks® Durasoil®,

2)  A QC report for the above sample,

3)  A copy of the chain of custody, and

4)  An invoice for analytical services.

 

 

 

All analyses were completed satisfactorily and all QC samples were found to be within our control limits. If you have any questions or concerns, please feel free to give me a call. Thank you for choosing McCampbell Analytical Laboratories for your analytical needs.

 

 

Best regards,

 

  Angela Rydelius Laboratory Manager

McCampbell Analytical, Inc.

 

 

 

 

 

 

 

 

 

continue reading...

BLOCK ENVIRONMENTAL SERVICES

2451 Estand Way

Pleasant Hill, CA 94523-3911

(925) 682-7200

FAX (925) 686-0399

Company Name:

Comments /Special Instructions:

Contact Name: David Block

Address:

 

Phoae:

 

 

 

 

 

-

FAX :

 

 

 

 

 

 

Tum Around Time:

STD

Project Name:

 

Soilworks

 

 

Durasoil

 

Send Invoice To: David Block

Project Number:

P.O./Contract No:

 

 

Formula Placeholder

 

McCampbell Analytical, Inc.

1534 Willow Pass Rd

Pittsburg, CA 94565-1701

(925) 252-9262


CHAIN-OF-CUSTODY RECORD           Page 1   of    1

 

WorkOrder: 0912166


ClientCode:BLPH

Formula Placeholder

 

 

Sample Receipt Checklist

 

 

Client Name:        BlockEnvironmental

 

Project Name:     Soil Works Durasoil


Date and Time Received:    12/7/2009 1:09:47 PM

 

Checklist completed and reviewed by:      Melissa Valles

 

 

WorkOrder N°:     0912166              Matrix Oil                                                     Carrier:       Client Drop-In

 

Chain of Custody (COC) Information

 Formula Placeholder

 

 

 

McCampbell Analytical, Inc.

"When Quality Counts"

1534 Willow Pass Road, Pittsburg, CA 94565-1701 Web: www.mccampbell.com      E-mail: main@mccampbell.com

Telephone: 877-252-9262     Fax: 925-252-9269

Block Environmental

2451 Estand Way Pleasant Hill, CA 94523

Client Project ID: Soil Works Durasoil

Date Sampled:    <Not Provided>

Date Received: 12/07/09

Client Contact: David Block

Date Extracted:

12/07/09

 

 

Client P.O.:

Date Analyzed

12/08/09

 

 

 

 

Extraction Method:

 

 

SW5030B

VolatileOrganicsbyP&TandGC/MS(BasicTargetList)*

Analytical Method:     SW8260B

 

 

Work Order:

 

 

0912166

 

Lab ID

0912166-001A

Client ID

Durasoil

Matrix

Oil

Compound

Concentration *

DF

Reporting

Limit

Compound

Concentration *

DF

Reporting

Limit

Acetone

ND

1.0

50

tert-Amyl methyl ether (TAME)

ND

1.0

5.0

Benzene

ND

1.0

5.0

Bromobenzene

ND

1.0

5.0

Bromochloromethane

ND

1.0

5.0

Bromodichloromethane

ND

1.0

5.0

Bromoform

ND

1.0

5.0

Bromomethane

ND

1.0

5.0

2-Butanone (MEK)

ND

1.0

20

t-Butyl alcohol (TBA)

ND

1.0

50

n-Butyl benzene

ND

1.0

5.0

sec-Butyl benzene

ND

1.0

5.0

tert-Butyl benzene

ND

1.0

5.0

Carbon Disulfide

ND

1.0

5.0

Carbon Tetrachloride

ND

1.0

5.0

Chlorobenzene

ND

1.0

5.0

Chloroethane

ND

1.0

5.0

Chloroform

ND

1.0

5.0

Chloromethane

ND

1.0

5.0

2-Chlorotoluene

ND

1.0

5.0

4-Chlorotoluene

ND

1.0

5.0

Dibromochloromethane

ND

1.0

5.0

1,2-Dibromo-3-chloropropane

ND

1.0

5.0

1,2-Dibromoethane (EDB)

ND

1.0

5.0

Dibromomethane

ND

1.0

5.0

1,2-Dichlorobenzene

ND

1.0

5.0

1,3-Dichlorobenzene

ND

1.0

5.0

1,4-Dichlorobenzene

ND

1.0

5.0

Dichlorodifluoromethane

ND

1.0

5.0

1,1-Dichloroethane

ND

1.0

5.0

1,2-Dichloroethane   (1,2-DCA)

ND

1.0

5.0

1,1-Dichloroethene

ND

1.0

5.0

cis-1,2-Dichloroethene

ND

1.0

5.0

trans-1,2-Dichloroethene

ND

1.0

5.0

1,2-Dichloropropane

ND

1.0

5.0

1,3-Dichloropropane

ND

1.0

5.0

2,2-Dichloropropane

ND

1.0

5.0

1,1-Dichloropropene

ND

1.0

5.0

cis-1,3-Dichloropropene

ND

1.0

5.0

trans-1,3-Dichloropropene

ND

1.0

5.0

Diisopropyl ether (DIPE)

ND

1.0

5.0

Ethylbenzene

ND

1.0

5.0

Ethyl tert-butyl ether (ETBE)

ND

1.0

5.0

Freon 113

ND

1.0

100

Hexachlorobutadiene

ND

1.0

5.0

Hexachloroethane

ND

1.0

5.0

2-Hexanone

ND

1.0

5.0

Isopropylbenzene

ND

1.0

5.0

4-Isopropyl toluene

ND

1.0

5.0

Methyl-t-butyl ether (MTBE)

ND

1.0

5.0

Methylene chloride

ND

1.0

5.0

4-Methyl-2-pentanone    (MIBK)

ND

1.0

5.0

Naphthalene

ND

1.0

5.0

n-Propyl benzene

ND

1.0

5.0

Styrene

ND

1.0

5.0

1,1,1,2-Tetrachloroethane

ND

1.0

5.0

1,1,2,2-Tetrachloroethane

ND

1.0

5.0

Tetrachloroethene

ND

1.0

5.0

Toluene

ND

1.0

5.0

1,2,3-Trichlorobenzene

ND

1.0

5.0

1,2,4-Trichlorobenzene

ND

1.0

5.0

1,1,1-Trichloroethane

ND

1.0

5.0

1,1,2-Trichloroethane

ND

1.0

5.0

Trichloroethene

ND

1.0

5.0

Trichlorofluoromethane

ND

1.0

5.0

1,2,3-Trichloropropane

ND

1.0

5.0

1,2,4-Trimethylbenzene

ND

1.0

5.0

1,3,5-Trimethylbenzene

ND

1.0

5.0

Vinyl Chloride

ND

1.0

5.0

Xylenes

ND

1.0

5.0

Surrogate Recoveries (%)

%SS1:

95

%SS2:

100

%SS3:

99

 

Comments:

* water and vapor samples are reported in µg/L, soil/sludge/solid samples in mg/kg, product/oil/non-aqueous liquid samples and all TCLP & SPLP extracts are reported in mg/L, wipe samples in µg/wipe.

 

ND means not detected above the reporting limit/method detection limit; N/A means analyte not applicable to this analysis. # surrogate diluted out of range or coelutes with another peak; &) low surrogate due to matrix interference.

                         

 

 

 

 

 

 

 

Angela Rydelius, Lab Manager

 

McCampbell Analytical, Inc.

"When Quality Counts"

1534 Willow Pass Road, Pittsburg, CA 94565-1701 Web: www.mccampbell.com      E-mail: main@mccampbell.com

Telephone: 877-252-9262     Fax: 925-252-9269

Block Environmental 2451 Estand Way

Pleasant Hill, CA 94523

Client Project ID: Soil Works Durasoil

Date Sampled:    <Not Provided>

Date Received: 12/07/09

Client Contact: David Block

Date Extracted:

12/07/09

 

Client P.O.:

Date Analyzed

12/09/09

 

 

 

Extraction Method:

 

 

SW3550C

Semi-VolatileOrganicsbyGC/MS(BasicTargetList)*

Analytical Method:    SW8270C

 

 

Work Order:

 

 

0912166

Lab ID

0912166-001A

Client ID

Durasoil

Matrix

Oil

Compound

Concentration *

DF

Reporting Limit

Compound

Concentration *

DF

Reporting Limit

Acenaphthene

ND<10,000

50

200

Acenaphthylene

ND<10,000

50

200

Acetochlor

ND<10,000

50

200

Anthracene

ND<10,000

50

200

Benzidine

ND<50,000

50

1000

Benzoic Acid

ND<50,000

50

1000

Benzo(a)anthracene

ND<10,000

50

200

Benzo(b)fluoranthene

ND<10,000

50

200

Benzo(k)fluoranthene

ND<10,000

50

200

Benzo(g,h,i)perylene

ND<10,000

50

200

Benzo(a)pyrene

ND<10,000

50

200

Benzyl Alcohol

ND<50,000

50

1000

1,1-Biphenyl

ND<10,000

50

200

Bis (2-chloroethoxy) Methane

ND<10,000

50

200

Bis (2-chloroethyl) Ether

ND<10,000

50

200

Bis (2-chloroisopropyl) Ether

ND<10,000

50

200

Bis (2-ethylhexyl) Phthalate

ND<10,000

50

200

4-Bromophenyl Phenyl Ether

ND<10,000

50

200

Butylbenzyl Phthalate

ND<10,000

50

200

4-Chloroaniline

ND<20,000

50

400

4-Chloro-3-methylphenol

ND<10,000

50

200

2-Chloronaphthalene

ND<10,000

50

200

2-Chlorophenol

ND<10,000

50

200

4-Chlorophenyl Phenyl Ether

ND<10,000

50

200

Chrysene

ND<10,000

50

200

Dibenzo(a,h)anthracene

ND<10,000

50

200

Dibenzofuran

ND<10,000

50

200

Di-n-butyl   Phthalate

ND<10,000

50

200

1,2-Dichlorobenzene

ND<10,000

50

200

1,3-Dichlorobenzene

ND<10,000

50

200

1,4-Dichlorobenzene

ND<10,000

50

200

3,3-Dichlorobenzidine

ND<20,000

50

400

2,4-Dichlorophenol

ND<10,000

50

200

Diethyl Phthalate

ND<10,000

50

200

2,4-Dimethylphenol

ND<10,000

50

200

Dimethyl   Phthalate

ND<10,000

50

200

4,6-Dinitro-2-methylphenol

ND<50,000

50

1000

2,4-Dinitrophenol

ND<50,000

50

1000

2,4-Dinitrotoluene

ND<10,000

50

200

2,6-Dinitrotoluene

ND<10,000

50

200

Di-n-octyl   Phthalate

ND<10,000

50

200

1,2-Diphenylhydrazine

ND<10,000

50

200

Fluoranthene

ND<10,000

50

200

Fluorene

ND<10,000

50

200

Hexachlorobenzene

ND<10,000

50

200

Hexachlorobutadiene

ND<10,000

50

200

Hexachlorocyclopentadiene

ND<50,000

50

1000

Hexachloroethane

ND<10,000

50

200

Indeno (1,2,3-cd) pyrene

ND<10,000

50

200

Isophorone

ND<10,000

50

200

2-Methylnaphthalene

ND<10,000

50

200

2-Methylphenol   (o-Cresol)

ND<10,000

50

200

3 &/or 4-Methylphenol (m,p-Cres

ND<10,000

50

200

Naphthalene

ND<10,000

50

200

2-Nitroaniline

ND<50,000

50

1000

3-Nitroaniline

ND<50,000

50

1000

4-Nitroaniline

ND<50,000

50

1000

Nitrobenzene

ND<10,000

50

200

2-Nitrophenol

ND<50,000

50

1000

4-Nitrophenol

ND<50,000

50

1000

N-Nitrosodiphenylamine

ND<10,000

50

200

N-Nitrosodi-n-propylamine

ND<10,000

50

200

Pentachlorophenol

ND<50,000

50

1000

Phenanthrene

ND<10,000

50

200

Phenol

ND<10,000

50

200

Pyrene

ND<10,000

50

200

1,2,4-Trichlorobenzene

ND<10,000

50

200

2,4,5-Trichlorophenol

ND<10,000

50

200

2,4,6-Trichlorophenol

ND<10,000

50

200

 

Surrogate Recoveries (%)

%SS1:

59

%SS2:

46

%SS3:

61

%SS4:

67

%SS5:

---#

%SS6:

60

Comments: a3

* water samples in µg/L, soil/sludge/solid samples in mg/kg, wipe samples in µg/wipe, product/oil/non-aqueous liquid samples and all TCLP & SPLP extracts are reported in mg/L.

 

ND means not detected above the reporting limit/method detection limit; N/A means analyte not applicable to this analysis. #) surrogate diluted out of range; &) low or no surrogate due to matrix interference.

a3) sample diluted due to high organic content.

                         

 

 

Angela Rydelius, Lab Manager

 

 

 

QC SUMMARY REPORT FOR SW8260B

 

 

W.O. Sample Matrix: Oil


 

QC Matrix: Soil


 

BatchID: 47431


 

WorkOrder: 0912166

 

 

EPA Method SW8260B                           Extraction SW5030B                                                                                  Spiked Sample ID: 0912103-013A

 

Analyte

Sample

Spiked

MS

MSD

MS-MSD

LCS

LCSD

LCS-LCSD

Acceptance Criteria (%)

mg/Kg

mg/Kg

% Rec.

% Rec.

% RPD

% Rec.

% Rec.

% RPD

MS / MSD

RPD

LCS/LCSD

RPD

tert-Amyl methyl ether (TAME)

ND

0.050

76.2

76.5

0.475

74.1

76.6

3.23

70 - 130

30

70 - 130

30

Benzene

ND

0.050

93

93.7

0.793

88.8

94.1

5.80

70 - 130

30

70 - 130

30

t-Butyl alcohol (TBA)

ND

0.25

85.7

86.8

1.17

84.1

81.9

2.73

70 - 130

30

70 - 130

30

Chlorobenzene

ND

0.050

99

100

1.14

94.6

99

4.56

70 - 130

30

70 - 130

30

1,2-Dibromoethane (EDB)

ND

0.050

96.4

97.8

1.44

92.7

94.4

1.78

70 - 130

30

70 - 130

30

1,2-Dichloroethane   (1,2-DCA)

ND

0.050

88.3

88.9

0.716

83.9

87.9

4.62

70 - 130

30

70 - 130

30

1,1-Dichloroethene

ND

0.050

122

122

0

114

121

6.42

70 - 130

30

70 - 130

30

Diisopropyl ether (DIPE)

ND

0.050

86.2

86.5

0.420

82.1

86.4

5.12

70 - 130

30

70 - 130

30

Ethyl tert-butyl ether (ETBE)

ND

0.050

84.3

84.1

0.213

80.9

84.5

4.33

70 - 130

30

70 - 130

30

Methyl-t-butyl ether (MTBE)

ND

0.050

89.9

90.4

0.554

85.7

89.6

4.46

70 - 130

30

70 - 130

30

Toluene

ND

0.050

101

102

1.18

95.6

101

5.06

70 - 130

30

70 - 130

30

Trichloroethene

ND

0.050

117

117

0

107

115

6.61

70 - 130

30

70 - 130

30

%SS1:

86

0.13

96

96

0

95

94

0.273

70 - 130

30

70 - 130

30

%SS2:

109

0.13

106

106

0

105

105

0

70 - 130

30

70 - 130

30

%SS3:

107

0.013

101

101

0

101

101

0

70 - 130

30

70 - 130

30

All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: NONE

 

 

BATCH 47431 SUMMARY

 

Lab ID                          Date Sampled      Date Extracted


Date Analyzed


Lab ID                          Date Sampled      Date Extracted


Date Analyzed

 

 

 

 

 

 

QC SUMMARY REPORT FOR SW8270C

 

 

W.O. Sample Matrix: Oil


 

QC Matrix: Soil


 

BatchID: 47356


 

WorkOrder: 0912166

 

 

EPA Method SW8270C                           Extraction SW3550C                                                                                  Spiked Sample ID: 0912002-004A

 

Analyte

Sample

Spiked

MS

MSD

MS-MSD

LCS

LCSD

LCS-LCSD

Acceptance Criteria (%)

mg/Kg

mg/Kg

% Rec.

% Rec.

% RPD

% Rec.

% Rec.

% RPD

MS / MSD

RPD

LCS/LCSD

RPD

Acenaphthene

ND<33

2

NR

NR

NR

70.2

70

0.228

30 - 130

30

30 - 130

30

4-Chloro-3-methylphenol

ND<33

4

NR

NR

NR

77.8

72.1

7.60

30 - 130

30

30 - 130

30

2-Chlorophenol

ND<33

4

NR

NR

NR

77.4

79.9

3.15

30 - 130

30

30 - 130

30

1,4-Dichlorobenzene

ND<33

2

NR

NR

NR

74.7

76.4

2.33

30 - 130

30

30 - 130

30

2,4-Dinitrotoluene

ND<33

2

NR

NR

NR

70.3

66.9

4.94

30 - 130

30

30 - 130

30

4-Nitrophenol

ND<160

4

NR

NR

NR

47.3

47

0.488

30 - 130

30

30 - 130

30

N-Nitrosodi-n-propylamine

ND<33

2

NR

NR

NR

84.5

86.5

2.30

30 - 130

30

30 - 130

30

Pentachlorophenol

ND<160

4

NR

NR

NR

54.7

48

13.2

30 - 130

30

30 - 130

30

Phenol

ND<33

4

NR

NR

NR

70

72.6

3.63

30 - 130

30

30 - 130

30

Pyrene

ND<33

2

NR

NR

NR

75.9

72.4

4.65

30 - 130

30

30 - 130

30

1,2,4-Trichlorobenzene

ND<33

2

NR

NR

NR

82.5

78.8

4.52

30 - 130

30

30 - 130

30

%SS1:

57

200

64

74

14.0

91

94

4.12

30 - 130

30

30 - 130

30

%SS2:

50

200

76

86

12.7

92

95

3.87

30 - 130

30

30 - 130

30

%SS3:

69

200

80

94

15.9

102

99

3.04

30 - 130

30

30 - 130

30

%SS4:

96

200

101

111

9.35

87

92

4.58

30 - 130

30

30 - 130

30

%SS5:

87

200

78

91

15.4

99

95

4.88

30 - 130

30

30 - 130

30

%SS6:

---#

200

---#

---#

N/A

92

88

3.97

30 - 130

30

30 - 130

30

All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: NONE

 

 

BATCH 47356 SUMMARY

 

Lab ID                          Date Sampled      Date Extracted


Date Analyzed


Lab ID                          Date Sampled      Date Extracted


Date Analyzed

 

 

 

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