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Soilworks products are the industry’s top standard due to our insistence on creating high performance soil stabilization and dust control products that stand up to rigorous testing – both in the lab and in the field. Our commitment to quality and performance has led to our involvement and testing in hundreds of real-world situations. The following library of reports, presentations, specifications, approvals and other similar documents provide you, our customer, the transparency and dependable assurance that is expected from Soilworks.
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McCampbell Analytical, Inc. “When Quality Counts” |
1534 Willow Pass Road, Pittsburg, CA 94565-1701 Web: www.mccampbell.com E-mail: main@mccampbell.com Telephone: 877-252-9262 Fax: 925-252-9269 |
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Block Environmental 2451 Estand Way Pleasant Hill, CA 94523 |
Client Project ID: Soil Works Durasoil |
Date Sampled: |
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Date Received: 12/07/09 |
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Client Contact: David Block |
Date Reported: 12/11/09 |
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Client P.O.: |
Date Completed: 12/11/09 |
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WorkOrder: 0912166
December 11, 2009
Dear David:
Enclosed within are:
1) The results of the 1 analyzed sample from your project: Soilworks® Durasoil®,
2) A QC report for the above sample,
3) A copy of the chain of custody, and
4) An invoice for analytical services.
All analyses were completed satisfactorily and all QC samples were found to be within our control limits. If you have any questions or concerns, please feel free to give me a call. Thank you for choosing McCampbell Analytical Laboratories for your analytical needs.
Best regards,
Angela Rydelius Laboratory Manager
McCampbell Analytical, Inc.
2451 Estand Way
Pleasant Hill, CA 94523-3911
(925) 682-7200
FAX (925) 686-0399
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McCampbell Analytical, Inc.
1534 Willow Pass Rd
Pittsburg, CA 94565-1701
(925) 252-9262
CHAIN-OF-CUSTODY RECORD Page 1 of 1
WorkOrder: 0912166
ClientCode:BLPH
Sample Receipt Checklist
Client Name: BlockEnvironmental
Project Name: Soil Works Durasoil
Date and Time Received: 12/7/2009 1:09:47 PM
Checklist completed and reviewed by: Melissa Valles
WorkOrder N°: 0912166 Matrix Oil Carrier: Client Drop-In
Chain of Custody (COC) Information
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McCampbell Analytical, Inc. “When Quality Counts” |
1534 Willow Pass Road, Pittsburg, CA 94565-1701 Web: www.mccampbell.com E-mail: main@mccampbell.com Telephone: 877-252-9262 Fax: 925-252-9269 |
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Block Environmental 2451 Estand Way Pleasant Hill, CA 94523 |
Client Project ID: Soil Works Durasoil |
Date Sampled: <Not Provided> |
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Date Received: 12/07/09 |
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Client Contact: David Block |
Date Extracted: |
12/07/09 |
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Client P.O.: |
Date Analyzed |
12/08/09 |
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Extraction Method: |
SW5030B |
VolatileOrganicsbyP&TandGC/MS(BasicTargetList)* Analytical Method: SW8260B |
Work Order: |
0912166 |
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Lab ID |
0912166-001A |
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Client ID |
Durasoil |
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Matrix |
Oil |
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|
Compound |
Concentration * |
DF |
Reporting Limit |
Compound |
Concentration * |
DF |
Reporting Limit |
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|
Acetone |
ND |
1.0 |
50 |
tert-Amyl methyl ether (TAME) |
ND |
1.0 |
5.0 |
|||||
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Benzene |
ND |
1.0 |
5.0 |
Bromobenzene |
ND |
1.0 |
5.0 |
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Bromochloromethane |
ND |
1.0 |
5.0 |
Bromodichloromethane |
ND |
1.0 |
5.0 |
|||||
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Bromoform |
ND |
1.0 |
5.0 |
Bromomethane |
ND |
1.0 |
5.0 |
|||||
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2-Butanone (MEK) |
ND |
1.0 |
20 |
t-Butyl alcohol (TBA) |
ND |
1.0 |
50 |
|||||
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n-Butyl benzene |
ND |
1.0 |
5.0 |
sec-Butyl benzene |
ND |
1.0 |
5.0 |
|||||
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tert-Butyl benzene |
ND |
1.0 |
5.0 |
Carbon Disulfide |
ND |
1.0 |
5.0 |
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Carbon Tetrachloride |
ND |
1.0 |
5.0 |
Chlorobenzene |
ND |
1.0 |
5.0 |
|||||
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Chloroethane |
ND |
1.0 |
5.0 |
Chloroform |
ND |
1.0 |
5.0 |
|||||
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Chloromethane |
ND |
1.0 |
5.0 |
2-Chlorotoluene |
ND |
1.0 |
5.0 |
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4-Chlorotoluene |
ND |
1.0 |
5.0 |
Dibromochloromethane |
ND |
1.0 |
5.0 |
|||||
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1,2-Dibromo-3-chloropropane |
ND |
1.0 |
5.0 |
1,2-Dibromoethane (EDB) |
ND |
1.0 |
5.0 |
|||||
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Dibromomethane |
ND |
1.0 |
5.0 |
1,2-Dichlorobenzene |
ND |
1.0 |
5.0 |
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1,3-Dichlorobenzene |
ND |
1.0 |
5.0 |
1,4-Dichlorobenzene |
ND |
1.0 |
5.0 |
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Dichlorodifluoromethane |
ND |
1.0 |
5.0 |
1,1-Dichloroethane |
ND |
1.0 |
5.0 |
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1,2-Dichloroethane (1,2-DCA) |
ND |
1.0 |
5.0 |
1,1-Dichloroethene |
ND |
1.0 |
5.0 |
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cis-1,2-Dichloroethene |
ND |
1.0 |
5.0 |
trans-1,2-Dichloroethene |
ND |
1.0 |
5.0 |
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1,2-Dichloropropane |
ND |
1.0 |
5.0 |
1,3-Dichloropropane |
ND |
1.0 |
5.0 |
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2,2-Dichloropropane |
ND |
1.0 |
5.0 |
1,1-Dichloropropene |
ND |
1.0 |
5.0 |
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cis-1,3-Dichloropropene |
ND |
1.0 |
5.0 |
trans-1,3-Dichloropropene |
ND |
1.0 |
5.0 |
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Diisopropyl ether (DIPE) |
ND |
1.0 |
5.0 |
Ethylbenzene |
ND |
1.0 |
5.0 |
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Ethyl tert-butyl ether (ETBE) |
ND |
1.0 |
5.0 |
Freon 113 |
ND |
1.0 |
100 |
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Hexachlorobutadiene |
ND |
1.0 |
5.0 |
Hexachloroethane |
ND |
1.0 |
5.0 |
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2-Hexanone |
ND |
1.0 |
5.0 |
Isopropylbenzene |
ND |
1.0 |
5.0 |
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4-Isopropyl toluene |
ND |
1.0 |
5.0 |
Methyl-t-butyl ether (MTBE) |
ND |
1.0 |
5.0 |
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Methylene chloride |
ND |
1.0 |
5.0 |
4-Methyl-2-pentanone (MIBK) |
ND |
1.0 |
5.0 |
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Naphthalene |
ND |
1.0 |
5.0 |
n-Propyl benzene |
ND |
1.0 |
5.0 |
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Styrene |
ND |
1.0 |
5.0 |
1,1,1,2-Tetrachloroethane |
ND |
1.0 |
5.0 |
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1,1,2,2-Tetrachloroethane |
ND |
1.0 |
5.0 |
Tetrachloroethene |
ND |
1.0 |
5.0 |
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Toluene |
ND |
1.0 |
5.0 |
1,2,3-Trichlorobenzene |
ND |
1.0 |
5.0 |
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1,2,4-Trichlorobenzene |
ND |
1.0 |
5.0 |
1,1,1-Trichloroethane |
ND |
1.0 |
5.0 |
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1,1,2-Trichloroethane |
ND |
1.0 |
5.0 |
Trichloroethene |
ND |
1.0 |
5.0 |
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Trichlorofluoromethane |
ND |
1.0 |
5.0 |
1,2,3-Trichloropropane |
ND |
1.0 |
5.0 |
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1,2,4-Trimethylbenzene |
ND |
1.0 |
5.0 |
1,3,5-Trimethylbenzene |
ND |
1.0 |
5.0 |
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Vinyl Chloride |
ND |
1.0 |
5.0 |
Xylenes |
ND |
1.0 |
5.0 |
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Surrogate Recoveries (%) |
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%SS1: |
95 |
%SS2: |
100 |
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%SS3: |
99 |
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Comments: |
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* water and vapor samples are reported in µg/L, soil/sludge/solid samples in mg/kg, product/oil/non-aqueous liquid samples and all TCLP & SPLP extracts are reported in mg/L, wipe samples in µg/wipe.
ND means not detected above the reporting limit/method detection limit; N/A means analyte not applicable to this analysis. # surrogate diluted out of range or coelutes with another peak; &) low surrogate due to matrix interference. |
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Angela Rydelius, Lab Manager
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McCampbell Analytical, Inc. “When Quality Counts” |
1534 Willow Pass Road, Pittsburg, CA 94565-1701 Web: www.mccampbell.com E-mail: main@mccampbell.com Telephone: 877-252-9262 Fax: 925-252-9269 |
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Block Environmental 2451 Estand Way Pleasant Hill, CA 94523 |
Client Project ID: Soil Works Durasoil |
Date Sampled: <Not Provided> |
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Date Received: 12/07/09 |
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Client Contact: David Block |
Date Extracted: |
12/07/09 |
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Client P.O.: |
Date Analyzed |
12/09/09 |
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Extraction Method: |
SW3550C |
Semi-VolatileOrganicsbyGC/MS(BasicTargetList)* Analytical Method: SW8270C |
Work Order: |
0912166 |
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Lab ID |
0912166-001A |
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Client ID |
Durasoil |
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Matrix |
Oil |
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Compound |
Concentration * |
DF |
Reporting Limit |
Compound |
Concentration * |
DF |
Reporting Limit |
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Acenaphthene |
ND<10,000 |
50 |
200 |
Acenaphthylene |
ND<10,000 |
50 |
200 |
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Acetochlor |
ND<10,000 |
50 |
200 |
Anthracene |
ND<10,000 |
50 |
200 |
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Benzidine |
ND<50,000 |
50 |
1000 |
Benzoic Acid |
ND<50,000 |
50 |
1000 |
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Benzo(a)anthracene |
ND<10,000 |
50 |
200 |
Benzo(b)fluoranthene |
ND<10,000 |
50 |
200 |
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Benzo(k)fluoranthene |
ND<10,000 |
50 |
200 |
Benzo(g,h,i)perylene |
ND<10,000 |
50 |
200 |
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Benzo(a)pyrene |
ND<10,000 |
50 |
200 |
Benzyl Alcohol |
ND<50,000 |
50 |
1000 |
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1,1-Biphenyl |
ND<10,000 |
50 |
200 |
Bis (2-chloroethoxy) Methane |
ND<10,000 |
50 |
200 |
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Bis (2-chloroethyl) Ether |
ND<10,000 |
50 |
200 |
Bis (2-chloroisopropyl) Ether |
ND<10,000 |
50 |
200 |
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Bis (2-ethylhexyl) Phthalate |
ND<10,000 |
50 |
200 |
4-Bromophenyl Phenyl Ether |
ND<10,000 |
50 |
200 |
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Butylbenzyl Phthalate |
ND<10,000 |
50 |
200 |
4-Chloroaniline |
ND<20,000 |
50 |
400 |
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4-Chloro-3-methylphenol |
ND<10,000 |
50 |
200 |
2-Chloronaphthalene |
ND<10,000 |
50 |
200 |
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2-Chlorophenol |
ND<10,000 |
50 |
200 |
4-Chlorophenyl Phenyl Ether |
ND<10,000 |
50 |
200 |
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Chrysene |
ND<10,000 |
50 |
200 |
Dibenzo(a,h)anthracene |
ND<10,000 |
50 |
200 |
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Dibenzofuran |
ND<10,000 |
50 |
200 |
Di-n-butyl Phthalate |
ND<10,000 |
50 |
200 |
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1,2-Dichlorobenzene |
ND<10,000 |
50 |
200 |
1,3-Dichlorobenzene |
ND<10,000 |
50 |
200 |
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1,4-Dichlorobenzene |
ND<10,000 |
50 |
200 |
3,3-Dichlorobenzidine |
ND<20,000 |
50 |
400 |
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2,4-Dichlorophenol |
ND<10,000 |
50 |
200 |
Diethyl Phthalate |
ND<10,000 |
50 |
200 |
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2,4-Dimethylphenol |
ND<10,000 |
50 |
200 |
Dimethyl Phthalate |
ND<10,000 |
50 |
200 |
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4,6-Dinitro-2-methylphenol |
ND<50,000 |
50 |
1000 |
2,4-Dinitrophenol |
ND<50,000 |
50 |
1000 |
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2,4-Dinitrotoluene |
ND<10,000 |
50 |
200 |
2,6-Dinitrotoluene |
ND<10,000 |
50 |
200 |
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Di-n-octyl Phthalate |
ND<10,000 |
50 |
200 |
1,2-Diphenylhydrazine |
ND<10,000 |
50 |
200 |
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Fluoranthene |
ND<10,000 |
50 |
200 |
Fluorene |
ND<10,000 |
50 |
200 |
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Hexachlorobenzene |
ND<10,000 |
50 |
200 |
Hexachlorobutadiene |
ND<10,000 |
50 |
200 |
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Hexachlorocyclopentadiene |
ND<50,000 |
50 |
1000 |
Hexachloroethane |
ND<10,000 |
50 |
200 |
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Indeno (1,2,3-cd) pyrene |
ND<10,000 |
50 |
200 |
Isophorone |
ND<10,000 |
50 |
200 |
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2-Methylnaphthalene |
ND<10,000 |
50 |
200 |
2-Methylphenol (o-Cresol) |
ND<10,000 |
50 |
200 |
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3 &/or 4-Methylphenol (m,p-Cres |
ND<10,000 |
50 |
200 |
Naphthalene |
ND<10,000 |
50 |
200 |
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2-Nitroaniline |
ND<50,000 |
50 |
1000 |
3-Nitroaniline |
ND<50,000 |
50 |
1000 |
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4-Nitroaniline |
ND<50,000 |
50 |
1000 |
Nitrobenzene |
ND<10,000 |
50 |
200 |
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2-Nitrophenol |
ND<50,000 |
50 |
1000 |
4-Nitrophenol |
ND<50,000 |
50 |
1000 |
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N-Nitrosodiphenylamine |
ND<10,000 |
50 |
200 |
N-Nitrosodi-n-propylamine |
ND<10,000 |
50 |
200 |
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Pentachlorophenol |
ND<50,000 |
50 |
1000 |
Phenanthrene |
ND<10,000 |
50 |
200 |
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Phenol |
ND<10,000 |
50 |
200 |
Pyrene |
ND<10,000 |
50 |
200 |
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1,2,4-Trichlorobenzene |
ND<10,000 |
50 |
200 |
2,4,5-Trichlorophenol |
ND<10,000 |
50 |
200 |
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2,4,6-Trichlorophenol |
ND<10,000 |
50 |
200 |
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Surrogate Recoveries (%) |
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%SS1: |
59 |
%SS2: |
46 |
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%SS3: |
61 |
%SS4: |
67 |
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%SS5: |
—# |
%SS6: |
60 |
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Comments: a3 |
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* water samples in µg/L, soil/sludge/solid samples in mg/kg, wipe samples in µg/wipe, product/oil/non-aqueous liquid samples and all TCLP & SPLP extracts are reported in mg/L.
ND means not detected above the reporting limit/method detection limit; N/A means analyte not applicable to this analysis. #) surrogate diluted out of range; &) low or no surrogate due to matrix interference. a3) sample diluted due to high organic content. |
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Angela Rydelius, Lab Manager
QC SUMMARY REPORT FOR SW8260B
W.O. Sample Matrix: Oil
QC Matrix: Soil
BatchID: 47431
WorkOrder: 0912166
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EPA Method SW8260B Extraction SW5030B Spiked Sample ID: 0912103-013A |
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Analyte |
Sample |
Spiked |
MS |
MSD |
MS-MSD |
LCS |
LCSD |
LCS-LCSD |
Acceptance Criteria (%) |
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|
mg/Kg |
mg/Kg |
% Rec. |
% Rec. |
% RPD |
% Rec. |
% Rec. |
% RPD |
MS / MSD |
RPD |
LCS/LCSD |
RPD |
|
|
tert-Amyl methyl ether (TAME) |
ND |
0.050 |
76.2 |
76.5 |
0.475 |
74.1 |
76.6 |
3.23 |
70 – 130 |
30 |
70 – 130 |
30 |
|
Benzene |
ND |
0.050 |
93 |
93.7 |
0.793 |
88.8 |
94.1 |
5.80 |
70 – 130 |
30 |
70 – 130 |
30 |
|
t-Butyl alcohol (TBA) |
ND |
0.25 |
85.7 |
86.8 |
1.17 |
84.1 |
81.9 |
2.73 |
70 – 130 |
30 |
70 – 130 |
30 |
|
Chlorobenzene |
ND |
0.050 |
99 |
100 |
1.14 |
94.6 |
99 |
4.56 |
70 – 130 |
30 |
70 – 130 |
30 |
|
1,2-Dibromoethane (EDB) |
ND |
0.050 |
96.4 |
97.8 |
1.44 |
92.7 |
94.4 |
1.78 |
70 – 130 |
30 |
70 – 130 |
30 |
|
1,2-Dichloroethane (1,2-DCA) |
ND |
0.050 |
88.3 |
88.9 |
0.716 |
83.9 |
87.9 |
4.62 |
70 – 130 |
30 |
70 – 130 |
30 |
|
1,1-Dichloroethene |
ND |
0.050 |
122 |
122 |
0 |
114 |
121 |
6.42 |
70 – 130 |
30 |
70 – 130 |
30 |
|
Diisopropyl ether (DIPE) |
ND |
0.050 |
86.2 |
86.5 |
0.420 |
82.1 |
86.4 |
5.12 |
70 – 130 |
30 |
70 – 130 |
30 |
|
Ethyl tert-butyl ether (ETBE) |
ND |
0.050 |
84.3 |
84.1 |
0.213 |
80.9 |
84.5 |
4.33 |
70 – 130 |
30 |
70 – 130 |
30 |
|
Methyl-t-butyl ether (MTBE) |
ND |
0.050 |
89.9 |
90.4 |
0.554 |
85.7 |
89.6 |
4.46 |
70 – 130 |
30 |
70 – 130 |
30 |
|
Toluene |
ND |
0.050 |
101 |
102 |
1.18 |
95.6 |
101 |
5.06 |
70 – 130 |
30 |
70 – 130 |
30 |
|
Trichloroethene |
ND |
0.050 |
117 |
117 |
0 |
107 |
115 |
6.61 |
70 – 130 |
30 |
70 – 130 |
30 |
|
%SS1: |
86 |
0.13 |
96 |
96 |
0 |
95 |
94 |
0.273 |
70 – 130 |
30 |
70 – 130 |
30 |
|
%SS2: |
109 |
0.13 |
106 |
106 |
0 |
105 |
105 |
0 |
70 – 130 |
30 |
70 – 130 |
30 |
|
%SS3: |
107 |
0.013 |
101 |
101 |
0 |
101 |
101 |
0 |
70 – 130 |
30 |
70 – 130 |
30 |
|
All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: NONE |
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BATCH 47431 SUMMARY
Lab ID Date Sampled Date Extracted
Date Analyzed
Lab ID Date Sampled Date Extracted
Date Analyzed
QC SUMMARY REPORT FOR SW8270C
W.O. Sample Matrix: Oil
QC Matrix: Soil
BatchID: 47356
WorkOrder: 0912166
|
EPA Method SW8270C Extraction SW3550C Spiked Sample ID: 0912002-004A |
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|
Analyte |
Sample |
Spiked |
MS |
MSD |
MS-MSD |
LCS |
LCSD |
LCS-LCSD |
Acceptance Criteria (%) |
|||
|
mg/Kg |
mg/Kg |
% Rec. |
% Rec. |
% RPD |
% Rec. |
% Rec. |
% RPD |
MS / MSD |
RPD |
LCS/LCSD |
RPD |
|
|
Acenaphthene |
ND<33 |
2 |
NR |
NR |
NR |
70.2 |
70 |
0.228 |
30 – 130 |
30 |
30 – 130 |
30 |
|
4-Chloro-3-methylphenol |
ND<33 |
4 |
NR |
NR |
NR |
77.8 |
72.1 |
7.60 |
30 – 130 |
30 |
30 – 130 |
30 |
|
2-Chlorophenol |
ND<33 |
4 |
NR |
NR |
NR |
77.4 |
79.9 |
3.15 |
30 – 130 |
30 |
30 – 130 |
30 |
|
1,4-Dichlorobenzene |
ND<33 |
2 |
NR |
NR |
NR |
74.7 |
76.4 |
2.33 |
30 – 130 |
30 |
30 – 130 |
30 |
|
2,4-Dinitrotoluene |
ND<33 |
2 |
NR |
NR |
NR |
70.3 |
66.9 |
4.94 |
30 – 130 |
30 |
30 – 130 |
30 |
|
4-Nitrophenol |
ND<160 |
4 |
NR |
NR |
NR |
47.3 |
47 |
0.488 |
30 – 130 |
30 |
30 – 130 |
30 |
|
N-Nitrosodi-n-propylamine |
ND<33 |
2 |
NR |
NR |
NR |
84.5 |
86.5 |
2.30 |
30 – 130 |
30 |
30 – 130 |
30 |
|
Pentachlorophenol |
ND<160 |
4 |
NR |
NR |
NR |
54.7 |
48 |
13.2 |
30 – 130 |
30 |
30 – 130 |
30 |
|
Phenol |
ND<33 |
4 |
NR |
NR |
NR |
70 |
72.6 |
3.63 |
30 – 130 |
30 |
30 – 130 |
30 |
|
Pyrene |
ND<33 |
2 |
NR |
NR |
NR |
75.9 |
72.4 |
4.65 |
30 – 130 |
30 |
30 – 130 |
30 |
|
1,2,4-Trichlorobenzene |
ND<33 |
2 |
NR |
NR |
NR |
82.5 |
78.8 |
4.52 |
30 – 130 |
30 |
30 – 130 |
30 |
|
%SS1: |
57 |
200 |
64 |
74 |
14.0 |
91 |
94 |
4.12 |
30 – 130 |
30 |
30 – 130 |
30 |
|
%SS2: |
50 |
200 |
76 |
86 |
12.7 |
92 |
95 |
3.87 |
30 – 130 |
30 |
30 – 130 |
30 |
|
%SS3: |
69 |
200 |
80 |
94 |
15.9 |
102 |
99 |
3.04 |
30 – 130 |
30 |
30 – 130 |
30 |
|
%SS4: |
96 |
200 |
101 |
111 |
9.35 |
87 |
92 |
4.58 |
30 – 130 |
30 |
30 – 130 |
30 |
|
%SS5: |
87 |
200 |
78 |
91 |
15.4 |
99 |
95 |
4.88 |
30 – 130 |
30 |
30 – 130 |
30 |
|
%SS6: |
—# |
200 |
—# |
—# |
N/A |
92 |
88 |
3.97 |
30 – 130 |
30 |
30 – 130 |
30 |
|
All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: NONE |
||||||||||||
BATCH 47356 SUMMARY
Lab ID Date Sampled Date Extracted
Date Analyzed
Lab ID Date Sampled Date Extracted
Date Analyzed
Copyright Soilworks, LLC 2003-. All Rights Reserved. Soilworks®, Soiltac®, Gorilla-Snot®, and Durasoil®are registered trademarks of Soilworks, LCC.
Copyright Soilworks, LLC 2003-. All Rights Reserved. Soilworks®, Soiltac®, Gorilla-Snot®, and Durasoil® are registered trademarks of Soilworks, LCC.
