Curtis & Tompkins Ltd - Analytical Report - Durasoil

John Goyette, Senior Program Manager
2011-03-24
Curtis & Tomkins, Ltd.

Curtis & Tompkins, Ltd.

Analytical Laboratories, Since 1878

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Laboratory Job Number 226591

ANALYTICAL REPORT

 

 

Soilworks, LLC

 

Project: STANDARD

Location: Durasoil®

Level:II 

 

 

 

 

Sample ID               Lab ID DURASOIL            226591-001

 

This data package has been reviewed for technical correctness and completeness. Release of this data has been authorized by the Laboratory Manager or the Manager's designee, as verified by the following signature. The results contained in this report meet all requirements of NELAC and pertain only to those samples which were submitted for analysis. This report may be reproduced only in its entirety.

Signature:                                     Date: 03/24/2011

Senior Program Manager

NELAP # 01107CA

 

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CASE NARRATIVE

Laboratory number:        226591

Client:                  Soilworks, LLC

Location:                Durasoil

Request Date:            03/14/11

Samples Received:         03/14/11

 

This data package contains sample and QC results for one fluid sample, requested for the above referenced project on 03/14/11. The sample was received intact.    No Benzene or Napthalene were detected in the sample above the detection limit of 0.3 ppm.

 

Volatile Organics by GC/MS (EPA 8260B):

No analytical problems were encountered.

 

 

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7.0

 

COOLER RECEIPT CHECKLIST

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Purgeable Organics by GC/MS

Lab #:

226591

 

Location:

Durasoil

Client:

Soilworks,

LLC

Prep:

EPA 5030B

Project#:

STANDARD

 

Analysis:

EPA 8260B

Field ID:

DURASOIL

 

Diln Fac:

50.00

Lab ID:

226591-001

 

Batch#:

172873

Matrix:

Miscell.

 

Sampled:

03/08/11

Units:

mg/Kg

 

Received:

03/14/11

Basis:

as received

 

Analyzed:

03/17/11

 

Analyte

 

Result

RL

Benzene

ND

0.3

Naphthalene

ND

0.3

 

Surrogate

%REC

Limits

Dibromofluoromethane

87

79-120

1,2-Dichloroethane-d4

83

72-148

Toluene-d8

94

80-120

Bromofluorobenzene

87

78-130

 

ND= Not Detected RL= Reporting Limit

Page 1 of 1                                                                                                                           3.1

 

Purgeable Organics by GC/MS

Lab #:

226591

 

Location:

Durasoil

Client:

Soilworks,

LLC

Prep:

EPA 5030B

Project#:

STANDARD

 

Analysis:

EPA 8260B

Type:

BLANK

 

Diln Fac:

1.000

Lab ID:

QC584196

 

Batch#:

172873

Matrix:

Soil

 

Analyzed:

03/17/11

Units:

mg/Kg

 

 

 

 

Analyte

 

Result

RL

Benzene

ND

0.005

Naphthalene

ND

0.005

 

Surrogate

%REC

Limits

Dibromofluoromethane

90

79-120

1,2-Dichloroethane-d4

82

72-148

Toluene-d8

103

80-120

Bromofluorobenzene

91

78-130

 

ND= Not Detected RL= Reporting Limit

Page 1 of 1                                                                                                                                        4.1

 

Purgeable Organics by GC/MS

Lab #:

226591

 

Location:

Durasoil

Client:

Soilworks,

LLC

Prep:

EPA 5030B

Project#:

STANDARD

 

Analysis:

EPA 8260B

Matrix:

Soil

 

Batch#:

172873

Units:

ug/Kg

Analyzed:

03/17/11

Diln Fac:

1.000

 

 

 

 

 

Type:            BS                             Lab ID:          QC584197

 

Analyte

Spiked

Result

%REC

Limits

1,1-Dichloroethene

20.00

18.88

94

68-134

Benzene

20.00

18.80

94

80-128

Trichloroethene

20.00

18.36

92

75-130

Toluene

20.00

18.95

95

80-130

Chlorobenzene

20.00

19.73

99

80-126

 

Surrogate

%REC

Limits

Dibromofluoromethane

91

79-120

1,2-Dichloroethane-d4

82

72-148

Toluene-d8

96

80-120

Bromofluorobenzene

90

78-130

 

 

 

Type:            BSD                            Lab ID:          QC584198

 

Analyte

Spiked

Result

%REC

Limits

RPD

Lim

1,1-Dichloroethene

20.00

18.17

91

68-134

4

27

Benzene

20.00

19.30

96

80-128

3

20

Trichloroethene

20.00

19.04

95

75-130

4

20

Toluene

20.00

19.03

95

80-130

0

20

Chlorobenzene

20.00

18.74

94

80-126

5

20

 

Surrogate

%REC

Limits

Dibromofluoromethane

90

79-120

1,2-Dichloroethane-d4

79

72-148

Toluene-d8

96

80-120

Bromofluorobenzene

90

78-130

 

RPD= Relative Percent Difference

Page 1 of 1                                                                                                                                        5.0

 

Purgeable Organics by GC/MS

Lab #:

226591

 

Location:

Durasoil

Client:

Soilworks,

LLC

Prep:

EPA 5030B

Project#:

STANDARD

 

Analysis:

EPA 8260B

Field ID:

ZZZZZZZZZZ

 

Batch#:

172873

MSS Lab ID:

226679-001

 

Sampled:

03/16/11

Matrix:

Soil

 

Received:

03/17/11

Units:

ug/Kg

 

Analyzed:

03/17/11

Basis:

as received

 

 

 

 

 

 

Type:

MS

Diln

Fac:

0.9634

Lab ID:

QC584200

 

 

 

 

Analyte

MSS

Result

Spiked

Result

%REC

Limits

1,1-Dichloroethene

<0.5475

48.17

39.17

81

65-139

Benzene

<0.8919

48.17

40.23

84

69-125

Trichloroethene

<1.041

48.17

42.98

89

60-145

Toluene

<1.203

48.17

41.20

86

62-128

Chlorobenzene

<0.2688

48.17

39.36

82

56-127

 

Surrogate

%REC

Limits

Dibromofluoromethane

91

79-120

1,2-Dichloroethane-d4

78

72-148

Toluene-d8

96

80-120

Bromofluorobenzene

90

78-130

 

 

 

Type:

MSD

Diln

Fac:

0.9542

Lab ID:

QC584201

 

 

 

 

Analyte

Spiked

Result

%REC

Limits

RPD

Lim

1,1-Dichloroethene

47.71

40.35

85

65-139

4

38

Benzene

47.71

41.88

88

69-125

5

36

Trichloroethene

47.71

45.50

95

60-145

7

41

Toluene

47.71

43.67

92

62-128

7

41

Chlorobenzene

47.71

42.52

89

56-127

9

42

 

Surrogate

%REC

Limits

Dibromofluoromethane

87

79-120

1,2-Dichloroethane-d4

75

72-148

Toluene-d8

98

80-120

Bromofluorobenzene

91

78-130

 

 

 

 

RPD= Relative Percent Difference

Page 1 of 1                                                                                                                                        6.0

 

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