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Curtis & Tompkins, Ltd.
Analytical Laboratories, Since 1878
Laboratory Job Number 226591
ANALYTICAL REPORT
Project: STANDARD
Location: Durasoil®
Level:II
Sample ID Lab ID DURASOIL 226591-001
This data package has been reviewed for technical correctness and completeness. Release of this data has been authorized by the Laboratory Manager or the Manager’s designee, as verified by the following signature. The results contained in this report meet all requirements of NELAC and pertain only to those samples which were submitted for analysis. This report may be reproduced only in its entirety.
Signature: Date: 03/24/2011
Senior Program Manager
NELAP # 01107CA
CASE NARRATIVE
Laboratory number: 226591
Client: Soilworks, LLC
Location: Durasoil
Request Date: 03/14/11
Samples Received: 03/14/11
This data package contains sample and QC results for one fluid sample, requested for the above referenced project on 03/14/11. The sample was received intact. No Benzene or Napthalene were detected in the sample above the detection limit of 0.3 ppm.
Volatile Organics by GC/MS (EPA 8260B):
No analytical problems were encountered.
Page 1 of 1 #
7.0
COOLER RECEIPT CHECKLIST
|
Purgeable Organics by GC/MS |
||||
|
Lab #: |
226591 |
|
Location: |
Durasoil |
|
Client: |
Soilworks, |
LLC |
Prep: |
EPA 5030B |
|
Project#: |
STANDARD |
|
Analysis: |
EPA 8260B |
|
Field ID: |
DURASOIL |
|
Diln Fac: |
50.00 |
|
Lab ID: |
226591-001 |
|
Batch#: |
172873 |
|
Matrix: |
Miscell. |
|
Sampled: |
03/08/11 |
|
Units: |
mg/Kg |
|
Received: |
03/14/11 |
|
Basis: |
as received |
|
Analyzed: |
03/17/11 |
|
Analyte |
|
Result |
RL |
|
Benzene |
ND |
0.3 |
|
|
Naphthalene |
ND |
0.3 |
|
|
Surrogate |
%REC |
Limits |
|
Dibromofluoromethane |
87 |
79-120 |
|
1,2-Dichloroethane-d4 |
83 |
72-148 |
|
Toluene-d8 |
94 |
80-120 |
|
Bromofluorobenzene |
87 |
78-130 |
ND= Not Detected RL= Reporting Limit
Page 1 of 1 3.1
|
Purgeable Organics by GC/MS |
||||
|
Lab #: |
226591 |
|
Location: |
Durasoil |
|
Client: |
Soilworks, |
LLC |
Prep: |
EPA 5030B |
|
Project#: |
STANDARD |
|
Analysis: |
EPA 8260B |
|
Type: |
BLANK |
|
Diln Fac: |
1.000 |
|
Lab ID: |
QC584196 |
|
Batch#: |
172873 |
|
Matrix: |
Soil |
|
Analyzed: |
03/17/11 |
|
Units: |
mg/Kg |
|
|
|
|
Analyte |
|
Result |
RL |
|
Benzene |
ND |
0.005 |
|
|
Naphthalene |
ND |
0.005 |
|
|
Surrogate |
%REC |
Limits |
|
Dibromofluoromethane |
90 |
79-120 |
|
1,2-Dichloroethane-d4 |
82 |
72-148 |
|
Toluene-d8 |
103 |
80-120 |
|
Bromofluorobenzene |
91 |
78-130 |
ND= Not Detected RL= Reporting Limit
Page 1 of 1 4.1
|
Purgeable Organics by GC/MS |
||||
|
Lab #: |
226591 |
|
Location: |
Durasoil |
|
Client: |
Soilworks, |
LLC |
Prep: |
EPA 5030B |
|
Project#: |
STANDARD |
|
Analysis: |
EPA 8260B |
|
Matrix: |
Soil |
|
Batch#: |
172873 |
|
Units: |
ug/Kg |
Analyzed: |
03/17/11 |
|
|
Diln Fac: |
1.000 |
|
|
|
Type: BS Lab ID: QC584197
|
Analyte |
Spiked |
Result |
%REC |
Limits |
|
1,1-Dichloroethene |
20.00 |
18.88 |
94 |
68-134 |
|
Benzene |
20.00 |
18.80 |
94 |
80-128 |
|
Trichloroethene |
20.00 |
18.36 |
92 |
75-130 |
|
Toluene |
20.00 |
18.95 |
95 |
80-130 |
|
Chlorobenzene |
20.00 |
19.73 |
99 |
80-126 |
|
Surrogate |
%REC |
Limits |
|
Dibromofluoromethane |
91 |
79-120 |
|
1,2-Dichloroethane-d4 |
82 |
72-148 |
|
Toluene-d8 |
96 |
80-120 |
|
Bromofluorobenzene |
90 |
78-130 |
Type: BSD Lab ID: QC584198
|
Analyte |
Spiked |
Result |
%REC |
Limits |
RPD |
Lim |
|
1,1-Dichloroethene |
20.00 |
18.17 |
91 |
68-134 |
4 |
27 |
|
Benzene |
20.00 |
19.30 |
96 |
80-128 |
3 |
20 |
|
Trichloroethene |
20.00 |
19.04 |
95 |
75-130 |
4 |
20 |
|
Toluene |
20.00 |
19.03 |
95 |
80-130 |
0 |
20 |
|
Chlorobenzene |
20.00 |
18.74 |
94 |
80-126 |
5 |
20 |
|
Surrogate |
%REC |
Limits |
|
Dibromofluoromethane |
90 |
79-120 |
|
1,2-Dichloroethane-d4 |
79 |
72-148 |
|
Toluene-d8 |
96 |
80-120 |
|
Bromofluorobenzene |
90 |
78-130 |
RPD= Relative Percent Difference
Page 1 of 1 5.0
|
Purgeable Organics by GC/MS |
||||
|
Lab #: |
226591 |
|
Location: |
Durasoil |
|
Client: |
Soilworks, |
LLC |
Prep: |
EPA 5030B |
|
Project#: |
STANDARD |
|
Analysis: |
EPA 8260B |
|
Field ID: |
ZZZZZZZZZZ |
|
Batch#: |
172873 |
|
MSS Lab ID: |
226679-001 |
|
Sampled: |
03/16/11 |
|
Matrix: |
Soil |
|
Received: |
03/17/11 |
|
Units: |
ug/Kg |
|
Analyzed: |
03/17/11 |
|
Basis: |
as received |
|
|
|
|
Type: |
MS |
Diln |
Fac: |
0.9634 |
|
Lab ID: |
QC584200 |
|
|
|
|
Analyte |
MSS |
Result |
Spiked |
Result |
%REC |
Limits |
|
1,1-Dichloroethene |
<0.5475 |
48.17 |
39.17 |
81 |
65-139 |
|
|
Benzene |
<0.8919 |
48.17 |
40.23 |
84 |
69-125 |
|
|
Trichloroethene |
<1.041 |
48.17 |
42.98 |
89 |
60-145 |
|
|
Toluene |
<1.203 |
48.17 |
41.20 |
86 |
62-128 |
|
|
Chlorobenzene |
<0.2688 |
48.17 |
39.36 |
82 |
56-127 |
|
|
Surrogate |
%REC |
Limits |
|
Dibromofluoromethane |
91 |
79-120 |
|
1,2-Dichloroethane-d4 |
78 |
72-148 |
|
Toluene-d8 |
96 |
80-120 |
|
Bromofluorobenzene |
90 |
78-130 |
|
Type: |
MSD |
Diln |
Fac: |
0.9542 |
|
Lab ID: |
QC584201 |
|
|
|
|
Analyte |
Spiked |
Result |
%REC |
Limits |
RPD |
Lim |
|
1,1-Dichloroethene |
47.71 |
40.35 |
85 |
65-139 |
4 |
38 |
|
Benzene |
47.71 |
41.88 |
88 |
69-125 |
5 |
36 |
|
Trichloroethene |
47.71 |
45.50 |
95 |
60-145 |
7 |
41 |
|
Toluene |
47.71 |
43.67 |
92 |
62-128 |
7 |
41 |
|
Chlorobenzene |
47.71 |
42.52 |
89 |
56-127 |
9 |
42 |
|
Surrogate |
%REC |
Limits |
|
Dibromofluoromethane |
87 |
79-120 |
|
1,2-Dichloroethane-d4 |
75 |
72-148 |
|
Toluene-d8 |
98 |
80-120 |
|
Bromofluorobenzene |
91 |
78-130 |
RPD= Relative Percent Difference
Page 1 of 1 6.0
Copyright Soilworks, LLC 2003-. All Rights Reserved. Soilworks®, Soiltac®, Gorilla-Snot®, and Durasoil®are registered trademarks of Soilworks, LCC.
Copyright Soilworks, LLC 2003-. All Rights Reserved. Soilworks®, Soiltac®, Gorilla-Snot®, and Durasoil® are registered trademarks of Soilworks, LCC.
